Syntheses and structures of a stable gallole free of Lewis base coordination and its dianion

Agou, Tomohiro; Wasano, Tatsuya; Sasamori, Takahiro; Tokitoh, Norihiro

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http://hdl.handle.net/2433/198687

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DCフィールド	値	言語
dc.contributor.author	Agou, Tomohiro	en
dc.contributor.author	Wasano, Tatsuya	en
dc.contributor.author	Sasamori, Takahiro	en
dc.contributor.author	Tokitoh, Norihiro	en
dc.contributor.alternative	吾郷, 友宏	ja
dc.contributor.alternative	時任, 宣博	ja
dc.date.accessioned	2015-07-08T08:04:22Z	-
dc.date.available	2015-07-08T08:04:22Z	-
dc.date.issued	2014-09-09	-
dc.identifier.issn	0894-3230	-
dc.identifier.uri	http://hdl.handle.net/2433/198687	-
dc.description.abstract	A stable Lewis base-free gallole bearing a bulky Mes[] group (=2, 4, 6-(t-Bu)[3]C[6]H[2]) was synthesized by the treatment of Mes[]GaCl[2] with a 3, 6-dilithio-3, 5-octadiene derivative. Reduction of the gallole with lithium metal afforded the corresponding gallole dianion species as a lithium salt. Structures of the gallole and the lithium salt of the gallole dianion have been elucidated by using X-ray crystallographic analysis, NMR spectroscopies, and density functional theory calculations	en
dc.format.mimetype	application/pdf	-
dc.language.iso	eng	-
dc.publisher	wiley	en
dc.rights	This is the peer reviewed version of the following article: Agou T., Wasano T., Sasamori T. and Tokitoh N., (2015), Syntheses and structures of a stable gallole free of Lewis base coordination and its dianion, J. Phys. Org. Chem., 28, 104–107, which has been published in final form at http://dx.doi.org/10.1002/poc.3344. This article may be used for non-commercial purposes in accordance with Wiley Terms and Conditions for Self-Archiving.	en
dc.rights	許諾条件により本文ファイルは2015-09-09に公開.	ja
dc.rights	この論文は出版社版でありません。引用の際には出版社版をご確認ご利用ください。	ja
dc.rights	This is not the published version. Please cite only the published version.	en
dc.subject	heteroles of heavier group 13 elements	en
dc.subject	gallole	en
dc.subject	gallole dianions	en
dc.subject	X-ray crystallographic analysis	en
dc.title	Syntheses and structures of a stable gallole free of Lewis base coordination and its dianion	en
dc.type	journal article	-
dc.type.niitype	Journal Article	-
dc.identifier.ncid	AA1068044X	-
dc.identifier.jtitle	Journal of Physical Organic Chemistry	en
dc.identifier.volume	28	-
dc.identifier.issue	2	-
dc.identifier.spage	104	-
dc.identifier.epage	107	-
dc.relation.doi	10.1002/poc.3344	-
dc.textversion	author	-
dc.startdate.bitstreamsavailable	2015-09-09	-
dcterms.accessRights	open access	-
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